2FOZ

human ADP-ribosylhydrolase 3

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	EMBL/DESY, HAMBURG BEAMLINE BW7A
Synchrotron site	EMBL/DESY, HAMBURG
Beamline	BW7A
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Wavelength(s)	1.1
Spacegroup name	P 21 21 21
Unit cell lengths	56.300, 60.400, 97.200
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.000 - 1.600
R-factor	0.17531
Rwork	0.175
R-free	0.20894
Structure solution method	SAD
RMSD bond length	0.012
RMSD bond angle	1.342
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	SHELXS
Refinement software	REFMAC (5.2.0005)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	99.000	1.630
High resolution limit [Å]	1.600	1.600
Number of reflections	44141
Completeness [%]	99.4	99.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1