Experimental procedure
| Temperature [K] | 277 |
| Collection date | 1975-02 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 61.630, 61.630, 70.980 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 10.000 - 1.800 |
| R-factor | 0.195 |
| Rwork | 0.195 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 23.370 * |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 10.000 |
| High resolution limit [Å] | 1.800 |
| Number of reflections | 14368 |
| Completeness [%] | 99.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 6.8 * | 4 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | ammonium sulfate | 2.5-2.8 (M) | |
| 2 | 1 | reservoir | Tris-HCl | or phosphate |
