2FH4
C-terminal half of gelsolin soaked in EGTA at pH 8
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I711 |
Synchrotron site | MAX II |
Beamline | I711 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-07-11 |
Detector | MARRESEARCH |
Wavelength(s) | 0.970 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 84.112, 87.782, 155.747 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.360 - 3.000 |
R-factor | 0.2192 |
Rwork | 0.214 |
R-free | 0.30990 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.347 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.300 |
High resolution limit [Å] | 2.240 | 2.240 |
Number of reflections | 55955 | |
Completeness [%] | 100.0 | 99.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | micro batch under oil | 4.5 | 277 | PEG 8000, pH 4.5, micro batch under oil, temperature 277K |