2FGG

Crystal Structure of Rv2632c

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 5.0.2
Synchrotron site	ALS
Beamline	5.0.2
Temperature [K]	100
Detector technology	CCD
Collection date	2005-01-09
Detector	ADSC QUANTUM 4
Wavelength(s)	0.979259
Spacegroup name	I 21 21 21
Unit cell lengths	48.054, 47.510, 94.807
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.400 - 2.300
R-factor	0.22634
Rwork	0.224
R-free	0.26481
Structure solution method	SAD
RMSD bond length	0.011
RMSD bond angle	2.139
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	SOLVE
Refinement software	REFMAC (5.2.0005)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.300	2.300
Rmerge	0.066	0.066
Number of reflections	4800
<I/σ(I)>	43.2	43.2
Completeness [%]	72.4	94.7
Redundancy	10.6	10.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION	5.5	298	0.1M Sodium Cacodylate, 11.5% Isopropanol, pH 5.5, EVAPORATION, temperature 298K