2FCF
The crystal structure of the 7th PDZ domain of MPDZ (MUPP-1)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-11-18 |
Detector | MARRESEARCH |
Wavelength(s) | 0.90010 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.122, 43.801, 50.167 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.990 - 1.760 |
R-factor | 0.20937 |
Rwork | 0.208 |
R-free | 0.24396 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1n7f |
RMSD bond length | 0.013 |
RMSD bond angle | 1.503 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.990 | 1.850 |
High resolution limit [Å] | 1.760 | 1.760 |
Rmerge | 0.073 | 0.096 |
Number of reflections | 8968 | |
<I/σ(I)> | 9.57 | |
Completeness [%] | 95.0 | 96.3 |
Redundancy | 6.84 | 6.35 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 298 | 30% mPEG 2K, 0.10M KSCN, pH 7.4, VAPOR DIFFUSION, SITTING DROP, temperature 298K |