2F88
Solution NMR structure of domain 5 from the Pyaiella littoralis (PL) group II intron
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Varian | INOVA | 500 | |
| 2 | Varian | INOVA | 600 | |
| 3 | Bruker | AVANCE | 600 | |
| 4 | Bruker | AVANCE | 800 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 3 | 2D NOESY |
| 10 | 4 | 1 | 13C/15N HSQC |
| 11 | 4 | 1 | 13C/15N TROSY |
| 2 | 2 | 3 | 2D TOCSY |
| 3 | 2 | 1 | 3D_13C-separated_NOESY |
| 4 | 1 | 1 | 3D_15N-separated_NOESY |
| 5 | 3 | 1 | 3D 1H-13C-1H HCCH TOCSY |
| 6 | 3 | 1 | 3D 1H-13C-1H HCCH COSY |
| 7 | 3 | 1 | 3D 1H-13C-1H HCCH COSY TROSY |
| 8 | 3 | 1 | 3D HCCNH |
| 9 | 2 | 2 | 3D_13C-separated_ROESY |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 6.5 | 278 | |
| 2 | 6.5 | 298 | |
| 3 | 6.5 | 308 | |
| 4 | 6.5 | 318 |
Conformers
| Conformers Calculated Total Number | 30 |
| Conformers Submitted Total Number | 10 |
