2F3Y
Calmodulin/IQ domain complex
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | CAMD BEAMLINE GCPCC |
Synchrotron site | CAMD |
Beamline | GCPCC |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-03-10 |
Detector | MARRESEARCH |
Wavelength(s) | 0.95144, 1.24242, 0.95056, 0.91838 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 86.200, 30.960, 63.940 |
Unit cell angles | 90.00, 114.54, 90.00 |
Refinement procedure
Resolution | 24.370 - 1.450 |
R-factor | 0.189 |
Rwork | 0.189 |
R-free | 0.21900 |
Structure solution method | MAD |
RMSD bond length | 0.004 |
RMSD bond angle | 1.000 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.470 |
High resolution limit [Å] | 1.420 | 1.420 |
Rmerge | 0.042 | 0.233 |
Number of reflections | 28262 | |
Completeness [%] | 96.0 | 64.1 |
Redundancy | 2.4 | 1.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.3 | 298 | 32% PEG 4000, 50mM TRIS, 50 mM MgCl2, pH 8.3, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
1 | VAPOR DIFFUSION, HANGING DROP | 8.3 | 298 | 32% PEG 4000, 50mM TRIS, 50 mM MgCl2, pH 8.3, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
1 | VAPOR DIFFUSION, HANGING DROP | 8.3 | 298 | 32% PEG 4000, 50mM TRIS, 50 mM MgCl2, pH 8.3, VAPOR DIFFUSION, HANGING DROP, temperature 298K |