2F0A
Crystal Structure of Monomeric Uncomplexed form of Xenopus dishevelled PDZ domain
Experimental procedure
実験手法 | MAD |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-08-01 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9798, 0.9801, 0.9611 |
Spacegroup name | P 61 |
格子定数 [Å] | 89.834, 89.834, 82.471 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 19.450 - 1.800 |
R因子 | 0.21571 |
Rwork | 0.214 |
R-free | 0.25263 |
Structure solution method | MAD |
結合長の平均二乗偏差(RMSD) [Å] | 0.019 |
結合角の平均二乗偏差(RMSD) [度] | 1.696 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0005) |
Quality characteristics
Overall | |
分解能 [Å] (低) | 19.450 |
分解能 [Å] (高) | 1.800 |
独立反射数 | 34969 |
完全性 [%] | 100.0 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 6.7 | 297 | 1.4 M ammonium sulfate 0.1 M sodium cacodylate, pH 6.7, VAPOR DIFFUSION, HANGING DROP, temperature 297K |