Experimental procedure
| Detector technology | IMAGE PLATE |
| Collection date | 1993-09-20 |
| Detector | MARRESEARCH |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 53.910, 23.100, 23.100 |
| Unit cell angles | 90.00, 110.40, 90.00 |
Refinement procedure
| Resolution | 26.000 * - 1.000 |
| R-factor | 0.1292 * |
| R-free | 0.16500 |
| RMSD bond length | 0.022 |
| RMSD bond angle | 0.022 |
| Data reduction software | MAR |
| Phasing software | SHELXL-93 |
| Refinement software | SHELXL-93 |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 8.000 * |
| High resolution limit [Å] | 1.000 |
| Rmerge | 0.054 |
| Total number of observations | 101188 * |
| Number of reflections | 13461 * |
| Completeness [%] | 92.4 * |
| Redundancy | 7.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 3.5 * | 298-301 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | Er-1 | 4.4 (mg/ml) | |
| 2 | 1 | drop | ammonium sulfate | 0.068 (M) | |
| 3 | 1 | drop | sodium citrate | 0.028 (M) | |
| 4 | 1 | drop | ethanol | 3.33 (%(v/v)) | pH3.50 |
| 5 | 1 | reservoir | ammonium sulfate | 0.12-0.15 (M) | |
| 6 | 1 | reservoir | sodium citrate | 0.05 (M) | pH3.50 |
| 7 | 1 | reservoir | ethanol | 6 (%(v/v)) |
