2ELC
Crystal structure of TTHA1842 from Thermus thermophilus HB8
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL26B1 |
Synchrotron site | SPring-8 |
Beamline | BL26B1 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2004-03-23 |
Detector | RIGAKU RAXIS V |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 165.319, 72.913, 141.263 |
Unit cell angles | 90.00, 125.21, 90.00 |
Refinement procedure
Resolution | 40.000 - 1.550 |
R-factor | 0.187 |
Rwork | 0.187 |
R-free | 0.20200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1v8g |
RMSD bond length | 0.007 |
RMSD bond angle | 1.300 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.610 |
High resolution limit [Å] | 1.550 | 1.550 |
Rmerge | 0.047 | 0.282 |
Number of reflections | 198639 | |
<I/σ(I)> | 12.9 | 4.9 |
Completeness [%] | 100.0 | 100 |
Redundancy | 3.9 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH | 5.6 | 295 | 3.85M Na Formic acid, 0.1M Citric acid, pH 5.6, Microbatch, temperature 295K |