2ELA
Crystal Structure of the PTB domain of human APPL1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4A |
Synchrotron site | NSLS |
Beamline | X4A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-06-19 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.97641 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 45.533, 61.593, 60.745 |
Unit cell angles | 90.00, 101.22, 90.00 |
Refinement procedure
Resolution | 29.790 - 2.000 |
R-factor | 0.222 |
Rwork | 0.222 |
R-free | 0.25900 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.300 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SnB |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.073 | 0.269 |
Number of reflections | 23819 | |
<I/σ(I)> | 16.74 | 3.917 |
Completeness [%] | 99.4 | 97 |
Redundancy | 3.6 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 277 | 0.1M sodium citrate (pH 5.6), 10% (w/v) PEG 10K, 10% (v/v) isopropanol, VAPOR DIFFUSION, SITTING DROP, temperature 277.0K |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 277 | 0.1M sodium citrate (pH 5.6), 10% (w/v) PEG 10K, 10% (v/v) isopropanol, VAPOR DIFFUSION, SITTING DROP, temperature 277.0K |