2EFD
Ara7/AtVps9a
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-04-23 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.91980 |
Spacegroup name | P 61 |
Unit cell lengths | 189.544, 189.544, 75.170 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.950 - 3.000 |
R-factor | 0.30797 |
Rwork | 0.306 |
R-free | 0.35126 |
Structure solution method | MAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.200 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 3.110 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.091 | 0.633 |
Number of reflections | 29805 | |
<I/σ(I)> | 27.6 | 3.5 |
Completeness [%] | 96.1 | 100 |
Redundancy | 11.2 | 10.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 289 | 3% PEG4000, 50mM imidazole malate, 50mM NaCl, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 289K |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 289 | 3% PEG4000, 50mM imidazole malate, 50mM NaCl, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 289K |