Experimental procedure
Source type | ROTATING ANODE |
Source details | SIEMENS |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Collection date | 1995-05-01 |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 73.500, 84.800, 80.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.800 |
R-factor | 0.193 |
Rwork | 0.193 |
R-free | 0.27600 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.897 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 10.000 |
High resolution limit [Å] | 2.800 |
Rmerge | 0.143 |
Number of reflections | 11995 |
Completeness [%] | 99.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.7 | pH 6.7 |