2EB9
Crystal Structure of Cu(II)(Sal-Leu)/apo-Myoglobin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2006-02-06 |
Detector | RIGAKU RAXIS VII |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 32.580, 57.901, 75.282 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 23.030 - 1.800 |
R-factor | 0.19162 |
Rwork | 0.189 |
R-free | 0.23948 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1v9q |
RMSD bond length | 0.016 |
RMSD bond angle | 1.477 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.091 | 0.266 |
Number of reflections | 13338 | |
<I/σ(I)> | 37.87 | |
Completeness [%] | 96.3 | 92.6 |
Redundancy | 9.7 | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.8 | 277 | 1.37M Sodium, Pottasium phosphate, pH 6.8, VAPOR DIFFUSION, HANGING DROP, temperature 277K |