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2E8Q

Structural study of Project ID PH0725 from Pyrococcus horikoshii OT3 (K19M)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2006-10-25
DetectorRIGAKU RAXIS VII
Wavelength(s)1.5418
Spacegroup nameP 41 21 2
Unit cell lengths104.693, 104.693, 137.942
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution26.870 - 2.500
R-factor0.211
Rwork0.210
R-free0.24000
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.008
RMSD bond angle1.400
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.590
High resolution limit [Å]2.5002.500
Rmerge0.0580.403
Number of reflections27146
<I/σ(I)>18.96.83
Completeness [%]99.9100
Redundancy13.313.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1MICROBATCH5.52913.85M Na Form, 0.1M Acet., pH 5.5, MICROBATCH, temperature 291K

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