2E75
Crystal Structure of the Cytochrome b6f Complex with 2-nonyl-4-hydroxyquinoline N-oxide (NQNO) from M.laminosus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-07-07 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97934 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 159.164, 159.164, 362.269 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.940 - 3.550 |
R-factor | 0.20396 |
Rwork | 0.201 |
R-free | 0.26705 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.038 |
RMSD bond angle | 4.076 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 137.360 |
High resolution limit [Å] | 3.550 |
Rmerge | 0.086 |
Number of reflections | 33633 |
Completeness [%] | 99.5 |
Redundancy | 9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |