2E6K
X-ray structure of Thermus thermopilus HB8 TT0505
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL26B1 |
Synchrotron site | SPring-8 |
Beamline | BL26B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-05-20 |
Detector | RIGAKU JUPITER 210 |
Wavelength(s) | 0.9, 0.97905, 0.9794 |
Spacegroup name | P 1 |
Unit cell lengths | 72.610, 88.960, 117.180 |
Unit cell angles | 72.48, 89.13, 73.36 |
Refinement procedure
Resolution | 38.590 - 2.090 |
R-factor | 0.217 |
Rwork | 0.217 |
R-free | 0.25900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1qgd |
RMSD bond length | 0.006 |
RMSD bond angle | 1.300 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | MOLREP |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.590 | 2.220 |
High resolution limit [Å] | 2.090 | 2.090 |
Rmerge | 0.061 | 0.190 |
Number of reflections | 154606 | |
<I/σ(I)> | 9.9 | 4.7 |
Completeness [%] | 97.7 | 97.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.8 | 298 | 10%(w/v) PEG 4000, 0.1M HEPES, pH 7.8, VAPOR DIFFUSION, SITTING DROP, temperature 298K |