2E2N
Crystal structure of Sulfolobus tokodaii hexokinase in the apo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Detector technology | CCD |
Collection date | 2005-02-15 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 82.897, 50.184, 83.269 |
Unit cell angles | 90.00, 114.69, 90.00 |
Refinement procedure
Resolution | 41.820 - 1.900 |
R-factor | 0.175 |
Rwork | 0.175 |
R-free | 0.21000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2e2o |
RMSD bond length | 0.005 |
RMSD bond angle | 1.100 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MERLOT |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.900 |
Number of reflections | 49689 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |