2E12
The crystal structure of XC5848 from Xanthomonas campestris adopting a novel variant of Sm-like motif
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL13B1 |
Synchrotron site | NSRRC |
Beamline | BL13B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-07-28 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.96437, 0.97983 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 49.942, 51.699, 82.120 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.700 |
R-factor | 0.24 |
Rwork | 0.220 |
R-free | 0.28000 |
Structure solution method | MAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.315 |
Data reduction software | DENZO |
Data scaling software | HKL-2000 |
Phasing software | AMoRE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.240 | 0.240 |
Number of reflections | 6937 | |
<I/σ(I)> | 8 | 7.9 |
Completeness [%] | 99.7 | 97.5 |
Redundancy | 4.5 | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 298 | pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K |