Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL38B1 |
| Synchrotron site | SPring-8 |
| Beamline | BL38B1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-05-22 |
| Detector | RIGAKU JUPITER 210 |
| Wavelength(s) | 0.9791, 0.9793, 0.9900 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 77.205, 123.219, 115.706 |
| Unit cell angles | 90.00, 104.36, 90.00 |
Refinement procedure
| Resolution | 47.570 - 2.100 |
| R-factor | 0.18526 |
| Rwork | 0.182 |
| R-free | 0.24321 |
| Structure solution method | MAD |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.265 |
| Data reduction software | JUPITOR210 |
| Data scaling software | HKL-2000 |
| Phasing software | SHELXD |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.570 | 2.180 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Number of reflections | 117625 | |
| Completeness [%] | 99.2 | 91.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
