2DK9
Solution structure of Calponin Homology domain of Human MICAL-1
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | DMX | 500 | |
| 2 | Bruker | DMX | 600 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 2 | 2D 1H-15N HSQC |
| 2 | 1 | 1 | 3D HNCO, HN(CA)CO, CBCA(CO)NH, CBCANH, C(CO)NH-TOCSY, H(CCO)NH-TOCSY, HBHA(CBCACO)NH,3D 15N-separted NOESY |
| 3 | 1 | 3 | 3D HCCH-TOCSY, HCCH-COSY, 13C-separted NOESY |
| 4 | 1 | 4 | 1H-coupled IPAP {15N, 1H}-HSQC |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 6.5 | 1 | 293 |
Conformers
| Conformers Calculated Total Number | 200 |
| Conformers Submitted Total Number | 20 |
