2DHE

CRYSTALLOGRAPHIC ANALYSIS OF THE CATALYTIC MECHANISM OF HALOALKANE DEHALOGENASE

Experimental procedure

Spacegroup name	P 21 21 2
Unit cell lengths	95.000, 72.600, 41.500
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	15.000 - 2.140 *
R-factor	0.165 *
RMSD bond length	0.009
RMSD bond angle	2.900
Refinement software	TNT

Data quality characteristics

	Overall
High resolution limit [Å]	2.140 *
Rmerge	0.057 *
Total number of observations	36467 *
Number of reflections	1284 *
Completeness [%]	84.7 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir		60 (%(w/v)sat)
2	1	reservoir	bis-Tris	100 (mM)