2DH3
Crystal Structure of human ED-4F2hc
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID13 |
Synchrotron site | ESRF |
Beamline | ID13 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-11-28 |
Detector | MARRESEARCH |
Wavelength(s) | 0.9789 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 69.497, 101.786, 121.966 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.000 - 2.800 |
R-factor | 0.21972 |
Rwork | 0.217 |
R-free | 0.27508 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.186 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.650 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 19650 | |
<I/σ(I)> | 15.74 | 3.46 |
Completeness [%] | 94.0 | 96.2 |
Redundancy | 7.1 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 298 | 25% PEG 3350, 0,2M AMMONIUM SULFATE, pH 6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |