2DFX
Crystal structure of the carboxy terminal domain of colicin E5 complexed with its inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | MACSCIENCE |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Collection date | 1998-11-24 |
Detector | MACSCIENCE |
Wavelength(s) | 1.5418 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 63.500, 74.400, 111.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.100 - 1.900 |
R-factor | 0.18 |
Rwork | 0.179 |
R-free | 0.19800 |
Structure solution method | MIR |
RMSD bond length | 0.005 |
RMSD bond angle | 1.300 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MLPHARE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.100 | 1.930 |
High resolution limit [Å] | 1.860 | 1.860 |
Number of reflections | 20556 | |
Completeness [%] | 92.7 | 91.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 2M ammonium sulfate, 0.1M TrisCl pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |