2D73
Crystal Structure Analysis of SusB
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-12-04 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 75.634, 112.340, 102.567 |
Unit cell angles | 90.00, 100.65, 90.00 |
Refinement procedure
Resolution | 15.000 - 1.600 |
Rwork | 0.177 |
R-free | 0.19800 |
Structure solution method | SAD |
RMSD bond length | 0.005 |
RMSD bond angle | 1.383 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SnB |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.660 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.068 | 0.417 |
Number of reflections | 235939 | |
<I/σ(I)> | 18.752 | 3.087 |
Completeness [%] | 99.8 | 97.7 |
Redundancy | 5.5 | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 298 | 10% PEG 8000, 0.1M imidazole, pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K |