2D5M
Flavoredoxin of Desulfovibrio vulgaris (Miyazaki F)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-10-05 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.71000 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 53.346, 53.346, 116.224 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 1.050 |
R-factor | 0.1352 |
Rwork | 0.128 |
R-free | 0.16150 |
Structure solution method | AB INITIO PHASING |
RMSD bond length | 0.016 |
RMSD bond angle | 0.031 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SHELX |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.090 |
High resolution limit [Å] | 1.050 | 1.050 |
Number of reflections | 89930 | |
Completeness [%] | 99.6 | 97 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 283 | PEG8K, Zn acetate, MES, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 283K |