2D51
Pentaketide chromone synthase (M207G mutant)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
| Synchrotron site | Photon Factory |
| Beamline | AR-NW12A |
| Detector technology | CCD |
| Collection date | 2005-01-27 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 1.00000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 74.320, 89.050, 70.670 |
| Unit cell angles | 90.00, 95.50, 90.00 |
Refinement procedure
| Resolution | 30.000 - 1.600 |
| Rwork | 0.192 |
| R-free | 0.20800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 1.600 |
| Number of reflections | 117664 |
| Completeness [%] | 97.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
