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2D4Y

Crystal structure of a 49K fragment of HAP1 (FlgK)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSPRING-8 BEAMLINE BL41XU
Synchrotron siteSPring-8
BeamlineBL41XU
Temperature [K]100
Detector technologyCCD
Collection date2003-02-06
DetectorMARRESEARCH
Wavelength(s)1.0394
Spacegroup nameP 21 21 21
Unit cell lengths88.928, 99.697, 109.645
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution74.540 - 2.100
R-factor0.22064
Rwork0.219
R-free0.25504
Structure solution methodMAD
RMSD bond length0.013
RMSD bond angle1.356
Data reduction softwareMOSFLM
Data scaling softwareCCP4 ((SCALA))
Phasing softwareSOLVE
Refinement softwareREFMAC (5.0)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]75.0002.210
High resolution limit [Å]2.1002.100
Rmerge0.0630.325
Number of reflections56302
<I/σ(I)>19.24.6
Completeness [%]97.897.7
Redundancy5.55.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION5.528914-15% PEG 8000, 20-25% isopropanol, 0.1M citrate, pH 5.5, VAPOR DIFFUSION, temperature 289K
1VAPOR DIFFUSION5.528914-15% PEG 8000, 20-25% isopropanol, 0.1M citrate, pH 5.5, VAPOR DIFFUSION, temperature 289K

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