2D4L
Crystal structure of truncated in C-terminal M-PMV dUTPase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | BW7B |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2005-01-19 |
Detector | MARRESEARCH |
Wavelength(s) | 0.843 |
Spacegroup name | P 63 |
Unit cell lengths | 61.163, 61.163, 64.167 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 1.700 |
R-factor | 0.1632 |
Rwork | 0.162 |
R-free | 0.17888 |
Starting model (for MR) | 2AKV |
RMSD bond length | 0.020 |
RMSD bond angle | 1.948 |
Data scaling software | XDS |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 53.000 | 1.800 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.037 | 0.533 |
Number of reflections | 14813 | |
<I/σ(I)> | 21.15 | 3.33 |
Completeness [%] | 98.3 | 98 |
Redundancy | 3.08 | 3.09 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | PEG 8000, AMMONIUM CHLORIDE, TRIS, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 293.0K |