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2D44

Crystal structure of arabinofuranosidase complexed with arabinofuranosyl-alpha-1,2-xylobiose

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-5A
Synchrotron sitePhoton Factory
BeamlineBL-5A
Temperature [K]100
Detector technologyCCD
Collection date2004-01-01
DetectorADSC QUANTUM 315
Wavelength(s)1.00000
Spacegroup nameP 21 21 21
Unit cell lengths39.530, 98.748, 143.946
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution46.700 - 2.300
R-factor0.203
Rwork0.203
R-free0.25000
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.006
RMSD bond angle1.400
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwareMOLREP
Refinement softwareCNS (1.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.380
High resolution limit [Å]2.3002.300
Number of reflections25910
Completeness [%]83.267
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP629830% PEG6000, 0.1M MES-NaOH, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K

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