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2D3I

Crystal Structure of Aluminum-Bound Ovotransferrin at 2.15 Angstrom Resolution

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSPRING-8 BEAMLINE BL38B1
Synchrotron siteSPring-8
BeamlineBL38B1
Temperature [K]100
Detector technologyCCD
Collection date2005-06-07
DetectorRIGAKU JUPITER 210
Wavelength(s)0.8
Spacegroup nameP 1 21 1
Unit cell lengths72.353, 59.184, 87.974
Unit cell angles90.00, 95.72, 90.00
Refinement procedure
Resolution49.030 - 2.150
R-factor0.206
Rwork0.206
R-free0.24300
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1ovt
RMSD bond length0.005
RMSD bond angle1.200
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwareCCP4
Refinement softwareCNS (1.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.230
High resolution limit [Å]2.1502.150
Number of reflections40021
<I/σ(I)>16.54.2
Completeness [%]98.494
Redundancy5.65.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP8277PEG400, pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 277K

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