2D2S
Crystal Structure of the Exo84p C-terminal Domains
Experimental procedure
Experimental method | MAD |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 54.850, 54.850, 209.130 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.000 - 2.850 |
R-factor | 0.273 |
Rwork | 0.269 |
R-free | 0.30600 |
Structure solution method | MAD |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 2.950 |
High resolution limit [Å] | 2.850 | 2.850 |
Number of reflections | 13025 | |
Completeness [%] | 97.5 | 57.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | PEG 3000, iso-propanol, sodium cloride, dithiothreitol, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |