2CZS
Crystal Structure Analysis of the Diheme c-type Cytochrome DHC2
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7A |
Synchrotron site | EMBL/DESY, Hamburg |
Beamline | BW7A |
Detector technology | CCD |
Collection date | 2004-07-20 |
Detector | MARRESEARCH |
Wavelength(s) | 0.9941, 1.7394, 1.7414 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 39.645, 55.679, 39.637 |
Unit cell angles | 90.00, 105.91, 90.00 |
Refinement procedure
Resolution | 38.120 - 1.500 |
R-factor | 0.22399 |
Rwork | 0.221 |
R-free | 0.27237 |
Structure solution method | MAD |
RMSD bond length | 0.014 |
RMSD bond angle | 1.581 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 38.120 |
High resolution limit [Å] | 1.500 |
Number of reflections | 26375 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |