Experimental procedure
| Detector technology | IMAGE PLATE |
| Detector | RIGAKU RAXIS IIC |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 40.700, 52.300, 90.400 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 6.000 - 1.640 |
| R-factor | 0.185 |
| Rwork | 0.185 |
| R-free | 0.22800 * |
| RMSD bond length | 0.013 |
| RMSD bond angle | 2.560 |
| Data reduction software | RIGAKU |
| Data scaling software | RIGAKU |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | Outer shell | |
| High resolution limit [Å] | 1.640 | 1.640 * |
| Rmerge | 0.051 | |
| Total number of observations | 55553 * | |
| Number of reflections | 21601 | |
| <I/σ(I)> | 1 | |
| Completeness [%] | 89.0 | 71.1 * |
| Redundancy | 2.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Microdialysis * | 8.5 * | 4 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | CyPA | 10-15 (mg/ml) | |
| 2 | 1 | 2 | Tris base | 20 (mM) | |
| 3 | 1 | 2 | EDTA | 2 (mM) | |
| 4 | 1 | 2 | 2-mercaptoethanol | 2 (mM) | |
| 5 | 1 | 2 | 0.5 (mM) | ||
| 6 | 1 | 2 | ethanol | 6.7 (%) | |
| 7 | 1 | 2 | PEG3350 | 11-13 (%) |
