2CW2
Crystal structure of Superoxide dismutase from P. Marinus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 53.813, 62.451, 57.354 |
Unit cell angles | 90.00, 95.54, 90.00 |
Refinement procedure
Resolution | 56.800 - 1.860 |
R-factor | 0.17309 |
Rwork | 0.171 |
R-free | 0.21560 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 1.313 |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.800 | 1.930 |
High resolution limit [Å] | 1.860 | 1.860 |
Rmerge | 0.046 | 0.295 |
Number of reflections | 32044 | |
Completeness [%] | 95.0 | 91 |
Redundancy | 5.5 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | VAPOR DIFFUSION, HANGING DROP |