2COV

Crystal structure of CBM31 from beta-1,3-xylanase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL45PX
Synchrotron site	SPring-8
Beamline	BL45PX
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2003-02-20
Detector	RIGAKU RAXIS V
Wavelength(s)	1.0000
Spacegroup name	P 21 21 21
Unit cell lengths	66.551, 78.290, 111.420
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 1.250
R-factor	0.15067
Rwork	0.149
R-free	0.17522
Structure solution method	SIRAS
RMSD bond length	0.024
RMSD bond angle	1.933
Refinement software	REFMAC (5.2.0005)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.250
Number of reflections	153374
Completeness [%]	95.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1