2CO6
Salmonella enterica SafA pilin in complex with the SafB chaperone (Type I)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 115.370, 40.822, 65.946 |
Unit cell angles | 90.00, 106.85, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.000 |
R-factor | 0.183 |
Rwork | 0.181 |
R-free | 0.22900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1l4i |
RMSD bond length | 0.014 |
RMSD bond angle | 1.591 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.100 | 0.290 |
Number of reflections | 20162 | |
<I/σ(I)> | 13.3 | 4 |
Completeness [%] | 99.9 | 100 |
Redundancy | 3.9 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 30% PEG 4000, 100 MM TRIS-HCL PH8.5, 200 MM SODIUM ACETATE, pH 8.50 |