2CO3
Salmonella enterica SafA pilin, head-to-tail swapped dimer of Ntd1 mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU R-AXIS |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 50.373, 41.216, 59.920 |
Unit cell angles | 90.00, 104.13, 90.00 |
Refinement procedure
Resolution | 15.000 - 1.780 |
R-factor | 0.1837 |
Rwork | 0.184 |
R-free | 0.21690 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.641 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHARP |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.840 |
High resolution limit [Å] | 1.780 | 1.780 |
Rmerge | 0.050 | 0.180 |
Number of reflections | 201192 | |
<I/σ(I)> | 22.8 | 5.1 |
Completeness [%] | 97.3 | 95.7 |
Redundancy | 2.9 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.6 | 30% PEG 4000, 100 MM MES, PH 5.6, 200 MM AMMONIUM ACETATE |