2CGA

BOVINE CHYMOTRYPSINOGEN A. X-RAY CRYSTAL STRUCTURE ANALYSIS AND REFINEMENT OF A NEW CRYSTAL FORM AT 1.8 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	59.300, 77.100, 110.100
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 1.800
R-factor	0.173 *
Rwork	0.173
RMSD bond length	0.016
RMSD bond angle	2.500
Refinement software	EREF

Data quality characteristics

	Overall
High resolution limit [Å]	1.800 *
Rmerge	0.086 *
Total number of observations	87718 *
Number of reflections	32818 *
Completeness [%]	69.0 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	ethanol	30 (%(v/v))
2	1	reservoir	phosphate	0.2 (M)
3	1	reservoir	bovine pancreatic trypsin inhibitor	2.5 (mg/cm3)