2CG7
SECOND AND THIRD FIBRONECTIN TYPE I MODULE PAIR (CRYSTAL FORM II).
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-02-18 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 52.651, 29.419, 51.009 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 52.630 - 1.200 |
R-factor | 0.19 |
Rwork | 0.189 |
R-free | 0.21900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2cg6 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.312 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.440 | 1.260 |
High resolution limit [Å] | 1.200 | 1.200 |
Rmerge | 0.060 | 0.320 |
Number of reflections | 167693 | |
<I/σ(I)> | 6.6 | 2.1 |
Completeness [%] | 97.5 | 96.8 |
Redundancy | 6.8 | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | WATER AND 0.02% SODIUM AZIDE, pH 7.00 |