2CE4
Manganese Superoxide Dismutase (Mn-SOD) from Deinococcus radiodurans
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 44.280, 83.210, 59.520 |
Unit cell angles | 90.00, 110.18, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.200 |
R-factor | 0.171 |
Rwork | 0.168 |
R-free | 0.23600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1vew |
RMSD bond length | 0.012 |
RMSD bond angle | 1.308 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.400 | 2.320 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.060 | 0.160 |
Number of reflections | 20567 | |
<I/σ(I)> | 15.6 | 6 |
Completeness [%] | 99.8 | 99.8 |
Redundancy | 3.4 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 10 MM TRIS-HCL PH 8.5, 20MM MNCL2, 30% PEG 4000 |