Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 52.900, 68.100, 34.900 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 * - 1.800 |
R-factor | 0.176 * |
Rwork | 0.176 |
RMSD bond length | 0.017 * |
RMSD bond angle | 0.031 * |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.800 * |
Rmerge | 0.043 * |
Total number of observations | 74360 * |
Number of reflections | 12162 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 2.0-2.5 (%(w/v)) | |
2 | 1 | drop | Tris-HCl | 50 (mM) | |
3 | 1 | drop | ethanol | 60-65 (%(v/v)) | |
4 | 1 | reservoir | ethanol | 70-75 (%(v/v)) |