Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 180 |
| Detector technology | CCD |
| Collection date | 2004-05-20 |
| Detector | ADSC CCD |
| Spacegroup name | P 42 21 2 |
| Unit cell lengths | 35.388, 35.384, 104.318 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 51.990 - 1.600 |
| R-factor | 0.219 |
| Rwork | 0.217 |
| R-free | 0.25900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | CrystalClear |
| Data scaling software | CrystalClear |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 34.770 |
| High resolution limit [Å] | 1.600 |
| Rmerge | 0.030 |
| Number of reflections | 9395 |
| <I/σ(I)> | 27.1 |
| Completeness [%] | 100.0 |
| Redundancy | 5.29 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 10.5 | 100MM CAPS PH 10.5, 30% PEG 400 |
