2CCE
Parallel Configuration of pLI E20S
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL11-1 |
| Synchrotron site | SSRL |
| Beamline | BL11-1 |
| Temperature [K] | 180 |
| Detector technology | CCD |
| Collection date | 2005-07-12 |
| Detector | ADSC CCD |
| Spacegroup name | P 41 3 2 |
| Unit cell lengths | 79.992, 79.992, 79.992 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 56.520 - 1.900 |
| R-factor | 0.284 |
| Rwork | 0.282 |
| R-free | 0.31900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.021 |
| RMSD bond angle | 1.546 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.900 |
| Rmerge | 0.060 |
| Number of reflections | 7118 |
| <I/σ(I)> | 20.6 |
| Completeness [%] | 100.0 |
| Redundancy | 10.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 2M NACL, 10% PEG 6K, pH 0.00 |
