Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | LURE BEAMLINE DW32 |
| Synchrotron site | LURE |
| Beamline | DW32 |
| Temperature [K] | 300 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 35.660, 73.420, 91.320 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 57.260 - 2.130 |
| R-factor | 0.169 |
| Rwork | 0.167 |
| R-free | 0.22400 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1bsg |
| RMSD bond length | 0.020 |
| RMSD bond angle | 1.923 |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 57.260 | 2.180 |
| High resolution limit [Å] | 2.130 | 2.130 |
| Rmerge | 0.060 | |
| Number of reflections | 11576 | |
| Completeness [%] | 86.9 | 53 |
| Redundancy | 2.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
