Experimental procedure
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL1-5 |
Synchrotron site | SSRL |
Beamline | BL1-5 |
Detector technology | AREA DETECTOR |
Collection date | 1986 |
Detector | XUONG-HAMLIN MULTIWIRE |
Wavelength(s) | 1.2359, 1.3771, 1.3790, 1.5416 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 30.880, 46.410, 65.570 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 7.000 - 1.800 |
R-factor | 0.141 * |
Rwork | 0.141 |
RMSD bond length | 0.013 |
RMSD bond angle | 0.027 |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
Rmerge | 0.043 |
Number of reflections | 43466 |
Completeness [%] | 89.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG6000 | 40 (%) | |
2 | 1 | reservoir | phosphate | 0.1 (M) |