2CB0
Crystal structure of glucosamine 6-phosphate deaminase from Pyrococcus furiosus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 4A |
Synchrotron site | PAL/PLS |
Beamline | 4A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-12-02 |
Detector | ADSC CCD |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 61.480, 93.890, 200.650 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.040 - 1.800 |
R-factor | 0.172 |
Rwork | 0.170 |
R-free | 0.21900 |
Structure solution method | OTHER |
RMSD bond length | 0.016 |
RMSD bond angle | 1.498 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 1.800 |
Rmerge | 0.080 |
Number of reflections | 40401 |
Completeness [%] | 74.0 |
Redundancy | 5.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | pH 6.00 |