2CAZ
ESCRT-I core
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-05-06 |
Detector | ADSC CCD |
Spacegroup name | P 61 |
Unit cell lengths | 167.914, 167.914, 50.242 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 145.860 - 3.600 |
R-factor | 0.329 |
Rwork | 0.328 |
R-free | 0.35700 |
Structure solution method | MAD |
RMSD bond length | 0.013 |
RMSD bond angle | 1.280 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SnB |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.000 | 3.800 |
High resolution limit [Å] | 3.600 | 3.600 |
Rmerge | 0.060 | 0.400 |
Number of reflections | 9610 | |
<I/σ(I)> | 24.21 | 1.8 |
Completeness [%] | 99.9 | 100 |
Redundancy | 7.7 | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 290 | 8-10% PEG 8000, 8-9% ETHYLENE GLYCOL, 0.1 M HEPES (PH 7.0- 8.0), 17 DEG C |