2C6U
Crystal structure of human CLEC-2 (CLEC1B)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX14.1 |
Synchrotron site | SRS |
Beamline | PX14.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-10-28 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 35.064, 55.065, 56.165 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.310 - 1.600 |
R-factor | 0.161 |
Rwork | 0.159 |
R-free | 0.19800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | COMPOSITE MODEL - SEE REMARKS |
RMSD bond length | 0.009 |
RMSD bond angle | 1.187 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CaspR |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.490 |
High resolution limit [Å] | 1.440 | 1.440 |
Rmerge | 0.040 | 0.110 |
Number of reflections | 20396 | |
<I/σ(I)> | 49.02 | 10.13 |
Completeness [%] | 88.0 | 24.4 |
Redundancy | 11.4 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 20% W/V POLYETHYLENE GLYCOL MONOMETHYL ETHER 5000 0.1M BIS-TRIS PH 6.5 |