2C6R
FE-SOAKED CRYSTAL STRUCTURE OF THE DPS92 FROM DEINOCOCCUS RADIODURANS
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-07-13 |
| Detector | ADSC CCD |
| Wavelength(s) | 1.1070,1.7399 |
| Spacegroup name | P 2 3 |
| Unit cell lengths | 88.965, 88.965, 88.965 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 89.090 - 2.100 |
| R-factor | 0.188 |
| Rwork | 0.188 |
| Structure solution method | SAD |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.422 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.660 | 2.050 |
| High resolution limit [Å] | 2.100 | 2.000 |
| Rmerge | 0.090 | 0.850 |
| Number of reflections | 13986 | |
| <I/σ(I)> | 16.9 | 1.7 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 7.3 | 7.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | 0.01M MGCL2, 0.05M TRIS PH7.5, 5% ISOPROPANOL, pH 7.50 |
